HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → Anisole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Acetone heptane | HCID 21879760 | — |
| Reactant | Methanol--water (1/1) | HCID 22242641 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Solvent | Nitromethane | HCID 6375 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Solvent | Methyl Isobutyl Ketone | HCID 7909 | — |
| Solvent | tert-Butyl methyl ether | HCID 15413 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Anisole | HCID 7519 | — |
| Product | Isopropyl Acetate | HCID 7915 | — |
Reaction Steps
In some embodiments, Form A was obtained from ethyl acetate, isopropyl acetate, tetrahydrofuran, methyl isobutyl ketone (MIBK), methyl ethyl ketone (MEK), nitromethane, methanol, ethanol, acetonitrile, dioxane, methyl tert-butyl ether (MTBE), anisole, acetone, heptanes, a methanol/water mixture or an acetone/heptane mixture. In some embodiments, Form A was obtained from ethyl acetate, isopropyl acetate, tetrahydrofuran, methyl isobutyl ketone (MIBK), methyl ethyl ketone (MEK), nitromethane, methanol, ethanol, acetonitrile, dioxane, methyl tert-butyl ether (MTBE), anisole, acetone, heptanes, or an acetone/heptane mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296753B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-686cd6958816481c94a3ba373e43cc8f |
| Source note | uspto-grants-2016_03 |