HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 89657740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 89656277 | HCID 89656277 | — |
| Product | HCID 89657740 | HCID 89657740 | — |
Reaction Steps
A mixture of Example 276 (0.50 g, 1.09 mmol) and thionyl chloride (5.0 mL, 69 mmol) was heated under reflux for 2 hours. The solvent was removed under reduced pressure and the residue was dried under vacuo for 1 hour to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296741B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-4e5f5dd0a68349f18d6d8fe6efe45801 |
| Source note | uspto-grants-2016_03 |