HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydroxyisobutyric acid → HCID 90014556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydroxyisobutyric acid | HCID 11671 | — |
| Reactant | HCID 90014477 | HCID 90014477 | — |
| Product | HCID 90014556 | HCID 90014556 | — |
Reaction Steps
10 mg (130 μmol) (RS)-6-{[7-(aminomethyl)-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4-yl]amino}-1,3-benzothiazol-2(3H)-one (prepared according to example 20) were transformed in analogy to example 23 using 2-hydroxy-2-methylpropanoic acid to give after working up and purification 23.8 mg (38%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296757B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-f048de1fa26c435599931b6d373210a7 |
| Source note | uspto-grants-2016_03 |