HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanesulfonyl chloride → HCID 90014761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanesulfonyl chloride | HCID 82408 | — |
| Reactant | HCID 90014477 | HCID 90014477 | — |
| Product | HCID 90014761 | HCID 90014761 | — |
Reaction Steps
75 mg (196 μmol) (RS)-6-{[7-(aminomethyl)-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4-yl]amino}-1,3-benzothiazol-2(3H)-one (prepared according to example 20), were transformed in analogy to example 21 using propane-2-sulfonyl chloride to give after working up and purification 5.7 mg (6%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296757B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-7b8ce7e271e5454faa7468ddf1140471 |
| Source note | uspto-grants-2016_03 |