HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(2-Methoxyethyl)amine → HCID 90014371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(2-Methoxyethyl)amine | HCID 2383 | — |
| Reactant | 4-Chloro-5,6,7,8-tetrahydrobenzo[4,5]thieno[2,3-d]pyrimidine-7-carboxylic acid | HCID 17990077 | — |
| Product | HCID 90014371 | HCID 90014371 | — |
Reaction Steps
300 mg (1.12 mmol) (RS)-4-chloro-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidine-7-carboxylic acid (prepared according to intermediate example 31b) were transformed in analogy to example 3 using 2-methoxy-N-(2-methoxyethyl)ethanamine to give after working up and purification 340 mg (79%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296757B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-032c9bf5001e4eb68472213357bb2e58 |
| Source note | uspto-grants-2016_03 |