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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 931129Generated: October 30, 2026

m-Chloroperbenzoic acid → HCID 89853680, compound

https://huagongshe.com/reaction/931129

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
ReactantEthyl 1-(pyridin-3-yl)cyclopropane-1-carboxylateHCID 21054369—
SolventDichloromethaneHCID 6344—
ProductHCID 89853680HCID 8985368058.1%

Reaction Steps

70% meta-Chloroperoxybenzoic acid (1.2 g, 4.9 mmol) was added to a solution of ethyl 1-(pyridin-3-yl)cyclopropanecarboxylate (400 mg, 2.4 mmol) in dichloromethane (5 mL) at room temperature and stirred for 16 h. The resulting precipitate was filtered and triturated with dichloromethane to afford the title compound (250 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09296745B2
Source datasetuspto-grants-2016_03
ORD IDord-296c5dbf1f554ca6914be0b18e3bee67
Source noteuspto-grants-2016_03