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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 931159Generated: November 3, 2026

Ethanol → HCID 117966583, compound

https://huagongshe.com/reaction/931159

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantSodiumHCID 5360545—
ReactantHCID 89853797HCID 89853797—
ProductHCID 117966583HCID 117966583—

Reaction Conditions

Temperature70 °C

Reaction Steps

Sodium metal (12 mg, 0.52 mmol) was added to anhydrous ethanol (3 mL) at room temperature and the mixture was stirred for 15 min. 1-(1H-pyrazol-1-yl)cyclopropanecarbonitrile (0.1 g, 0.75 mmol) dissolved in ethanol (2 mL) was added and the reaction mixture was heated to 70° C. for 90 min. The resulting solution was used without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09296745B2
Source datasetuspto-grants-2016_03
ORD IDord-3cabb66fe334417aa947b316315a861e
Source noteuspto-grants-2016_03