HRID931305
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Saturated ethereal hydrogen chloride (40 mL) was added to a solution of cis-tert-butyl 4-methyl-3-(pyrrolidine-1-carbonyl)piperidine-1-carboxylate (2.6 g, 8.78 mmol) in ether (20 mL) at 0° C. The reaction mixture was stirred at room temperature for 2 h. The solvent was removed under reduced pressure to afford cis-(4-methylpiperidin-3-yl)(pyrrolidin-1-yl)methanone (1.7 g).
WORKUP
后处理
- customThe solvent was removed under reduced pressure