HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Aminomethyl)-N-(3-pyridinyl)benzamide dihydrobromide → 4-(Aminomethyl)-N-(pyridin-3-YL)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Aminomethyl)-N-(3-pyridinyl)benzamide dihydrobromide | HCID 70654644 | — |
| Solvent | Ammonia | HCID 222 | — |
| Product | 4-(Aminomethyl)-N-(pyridin-3-YL)benzamide | HCID 16774572 | — |
Reaction Steps
A suspension of dihydrobromide salt 32 (1 mmol) in dilute aqueous ammonia solution (50 mL) was extracted into CHCl3 (3×50 mL), the organic fraction dried and the solvent evaporated to give crude benzamide 33 which was used directly.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296732B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-6340222ef3b54806b37de5b0be5160d1 |
| Source note | uspto-grants-2016_03 |