HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chlorophenyl)-2,7-dimethyl-6-vinylquinoline → (S)-1-(5-(4-chlorophenyl)-2,7-dimethylquinolin-6-yl)ethane-1,2-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chlorophenyl)-2,7-dimethyl-6-vinylquinoline | HCID 66631776 | — |
| Reactant | (S)-1-(7-chloro-5-(4-chlorophenyl)-2-methylquinolin-6-yl)ethane-1,2-diol | HCID 66633446 | — |
| Product | (S)-1-(5-(4-chlorophenyl)-2,7-dimethylquinolin-6-yl)ethane-1,2-diol | HCID 66633464 | — |
Reaction Steps
Compound 2G was prepared following the procedure used to prepare compound 1H of Example 1, except that 5-(4-chlorophenyl)-2,7-dimethyl-6-vinylquinoline (2F) was used instead of compound 1G. LCMS-ESI+ (m/z): 328.2, 330.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296758B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-316cad1d250d442ba4fb6de064a86422 |
| Source note | uspto-grants-2016_03 |