HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium ethoxide → HCID 66630478, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | HCID 66631437 | HCID 66631437 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66630478 | HCID 66630478 | — |
Reaction Steps
(S)-2-tert-Butoxy-2-(5-(4-chlorophenyl)-2-(ethoxymethyl)-7-methylquinolin-6-yl)ethanol was prepared following the procedure used to prepare compound (S)-2-tert-butoxy-2-(5-(4-chlorophenyl)-2-(methoxymethyl)-7-methylquinolin-6-yl)ethanol of Example 12, except that sodium ethoxide in ethanol solution was used instead of sodium methoxide in methanol solution. LCMS-ESI+ (m/z): 428.2, 430.2 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296758B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-2936ea01431e4781ae53742cdc9e17ba |
| Source note | uspto-grants-2016_03 |