Propanal → HCID 15668519, compound

HRID 932184Notes

Reaction equation

HRID 932184 reaction equation
Br[C:2]1[CH:7]=[CH:6][CH:5]=[C:4]([Br:8])[N:3]=1.[CH:9](=[O:12])[CH2:10][CH3:11].N1C=CC=CC=1C(O)CCC>>[Br:8][C:4]1[N:3]=[C:2]([CH:9]([OH:12])[CH2:10][CH3:11])[CH:7]=[CH:6][CH:5]=1

Participants

4

Reactant 3

HCID 527PropanalHCID 122742,6-DibromopyridineHCID 13926171HCID 13926171, compound

Product 1

HCID 15668519HCID 15668519, compound

Procedure

The title compound was prepared from 2,6-dibromopyridine (purchased from Sigma-Aldrich, St. Louis, Mo.) and propionaldehyde following a procedure similar to the one described above for the synthesis of 1-(pyridin-2-yl)butan-1-ol (Example 231, step A). Mass Spectrum (ESI) m/z=219.9 and 217.9 (M+1).

Sources & evidence

ORD record
ord-8d31d92dd2104ec78da31d2eda272b94
Source dataset
uspto-grants-2016_03
Patent number
US09296736B2

Reaction notes

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