Dimethylformamide → 7-Chloro-3-iodo-2-phenyl-pyrano[2,3-b]pyridin-4-one

HRID 938575Notes

Reaction equation

HRID 938575 reaction equation
[Cl:29][CH2:30][Cl:31].[I:1][c:2]1[c:3](=[O:19])[c:4]2[c:5]([nH:6][c:7](=[O:10])[cH:8][cH:9]2)[o:11][c:12]1-[c:13]1[cH:14][cH:15][cH:16][cH:17][cH:18]1.[O:20]=[CH:21][N:22]([CH3:23])[CH3:24].[S:25]([Cl:26])([Cl:27])=[O:28]>>[I:1][c:2]1[c:3](=[O:19])[c:4]2[c:5]([n:6][c:7]([Cl:27])[cH:8][cH:9]2)[o:11][c:12]1-[c:13]1[cH:14][cH:15][cH:16][cH:17][cH:18]1

Participants

5

Reactant 4

HCID 6228DimethylformamideHCID 6344DichloromethaneHCID 24386Thionyl ChlorideHCID 866710233-Iodo-2-phenyl-8H-pyrano[2,3-b]pyridine-4,7-dione

Product 1

HCID 866710247-Chloro-3-iodo-2-phenyl-pyrano[2,3-b]pyridin-4-one

Sources & evidence

ORD record
ord-49a3efff9a5b4bbb80d34dae0821fab1
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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