p-Toluenesulfonic acid → Ethyl 2,7-diazabicyclo[3.3.0]octane-2-carboxylate

HRID 938746Notes

Reaction equation

HRID 938746 reaction equation
[CH:1]12[N:2]([C:16](=[O:17])[O:18][CH2:19][CH3:20])[CH2:3][CH2:4][CH:5]1[CH2:6][N:7]([C:9]([O:10][C:11]([CH3:12])([CH3:13])[CH3:14])=[O:15])[CH2:8]2.[CH:32]([Cl:33])([Cl:34])[Cl:35].[c:21]1([CH3:22])[cH:23][cH:24][c:25]([S:26]([OH:27])(=[O:28])=[O:29])[cH:30][cH:31]1>>[CH:1]12[N:2]([C:16](=[O:17])[O:18][CH2:19][CH3:20])[CH2:3][CH2:4][CH:5]1[CH2:6][NH:7][CH2:8]2

Participants

4

Reactant 3

HCID 6101p-Toluenesulfonic acidHCID 6212ChloroformHCID 191009335-(1,1-Dimethylethyl) 1-ethyl hexahydropyrrolo[3,4-b]pyrrole-1,5-dicarboxylate

Product 1

HCID 15070028Ethyl 2,7-diazabicyclo[3.3.0]octane-2-carboxylate

Sources & evidence

ORD record
ord-5dc9fc6d8635406294521f886be06df9
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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