Dichloromethane → 6-[2-(Bromomethyl)-3-methylbutyl]-1-(3-methoxypropyl)indazole

HRID 942554Notes

Reaction equation

HRID 942554 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][n:6]1[n:7][cH:8][c:9]2[cH:10][cH:11][c:12]([CH2:15][CH:16]([CH2:17][OH:18])[CH:19]([CH3:20])[CH3:21])[cH:13][c:14]12.[Cl:49][CH2:50][Cl:51].[O:41]=[C:42]1[N:43]([Br:48])[C:44](=[O:45])[CH2:46][CH2:47]1.[c:22]1([P:23]([c:24]2[cH:25][cH:26][cH:27][cH:28][cH:29]2)[c:30]2[cH:31][cH:32][cH:33][cH:34][cH:35]2)[cH:36][cH:37][cH:38][cH:39][cH:40]1>>[CH3:1][O:2][CH2:3][CH2:4][CH2:5][n:6]1[n:7][cH:8][c:9]2[cH:10][cH:11][c:12]([CH2:15][CH:16]([CH2:17][Br:48])[CH:19]([CH3:20])[CH3:21])[cH:13][c:14]12

Participants

5

Reactant 4

HCID 6344DichloromethaneHCID 11776TriphenylphosphineHCID 67184N-bromobutanimideHCID 687813752-[[1-(3-Methoxypropyl)indazol-6-yl]methyl]-3-methylbutan-1-ol

Product 1

HCID 687832206-[2-(Bromomethyl)-3-methylbutyl]-1-(3-methoxypropyl)indazole

Sources & evidence

ORD record
ord-2816b569b2394d629c01c0d3fabf00fd
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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