Bromide ion → 1,4-Diacetylpiperidine

HRID 944252Notes

Reaction equation

HRID 944252 reaction equation
[Br-:16].[C:1]([CH3:2])(=[O:3])[N:4]1[CH2:5][CH2:6][CH:7]([C:10](=[O:11])[N:12]([O:13][CH3:14])[CH3:15])[CH2:8][CH2:9]1.[CH3:17][Mg+:18].[O:19]1[CH2:20][CH2:21][CH2:22][CH2:23]1>>[C:1]([CH3:2])(=[O:3])[N:4]1[CH2:5][CH2:6][CH:7]([C:10](=[O:11])[CH3:17])[CH2:8][CH2:9]1

Participants

5

Reactant 4

HCID 259Bromide ionHCID 8028TetrahydrofuranHCID 187135481-acetyl-N-methoxy-N-methylpiperidine-4-carboxamideHCID 178477777HCID 178477777, compound

Product 1

HCID 27772501,4-Diacetylpiperidine

Sources & evidence

ORD record
ord-17dedf5a61f3464791b644f4d438804f
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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