Benzyl Alcohol → 2-(Benzyloxy)-1,3-difluoro-5-nitrobenzene

HRID 952846Notes

Reaction equation

HRID 952846 reaction equation
[C:1](=[O:2])([O-:3])[O-:4].[CH3:27][N:28]([CH3:29])[CH:30]=[O:31].[F:7][c:8]1[c:9]([F:18])[c:10]([F:17])[cH:11][c:12]([N+:14](=[O:15])[O-:16])[cH:13]1.[K+:5].[K+:6].[OH:19][CH2:20][c:21]1[cH:22][cH:23][cH:24][cH:25][cH:26]1>>[F:7][c:8]1[c:9]([O:19][CH2:20][c:21]2[cH:22][cH:23][cH:24][cH:25][cH:26]2)[c:10]([F:17])[cH:11][c:12]([N+:14](=[O:15])[O-:16])[cH:13]1

Participants

6

Reactant 5

HCID 244Benzyl AlcoholHCID 813Potassium Cation2×HCID 6228DimethylformamideHCID 19660Carbonate IonHCID 27827931,2,3-Trifluoro-5-nitrobenzene

Product 1

HCID 231303422-(Benzyloxy)-1,3-difluoro-5-nitrobenzene

Sources & evidence

ORD record
ord-d01a7acaf067406eb9a9867ee5f56167
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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