Diethyl Ether → 3-phenyl-2,3-dihydro4H-1,4-benzoxazin-4-ylamine

HRID 957299Notes

Reaction equation

HRID 957299 reaction equation
[Al+3:2].[CH2:25]([O:26][CH2:27][CH3:28])[CH3:29].[H-:1].[H-:4].[H-:5].[H-:6].[Li+:3].[N:7](=[O:8])[N:9]1[CH:10]([c:19]2[cH:20][cH:21][cH:22][cH:23][cH:24]2)[CH2:11][O:12][c:13]2[c:14]1[cH:15][cH:16][cH:17][cH:18]2>>[NH2:7][N:9]1[CH:10]([c:19]2[cH:20][cH:21][cH:22][cH:23][cH:24]2)[CH2:11][O:12][c:13]2[c:14]1[cH:15][cH:16][cH:17][cH:18]2

Participants

6

Reactant 5

HCID 3283Diethyl EtherHCID 28486Lithium ionHCID 104727Aluminum CationHCID 166653Hydride4×HCID 121486174-Nitroso-3-phenyl-3,4-dihydro-2H-1,4-benzoxazine

Product 1

HCID 121486183-phenyl-2,3-dihydro4H-1,4-benzoxazin-4-ylamine

Sources & evidence

ORD record
ord-468ffdf4567d49569da833b76fe701cc
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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