Dichloromethane → 2-Bromoimidazo[5,1-b]thiazole-7-carbaldehyde

HRID 958166Notes

Reaction equation

HRID 958166 reaction equation
[Br:1][c:2]1[cH:3][n:4]2[c:5]([s:6]1)[c:7]([CH2:10][OH:11])[n:8][cH:9]2.[CH3:36][CH2:37][O:38][C:39](=[O:40])[CH3:41].[Cl:33][CH2:34][Cl:35].[Cr:12]([O:13][Cr:14]([O-:15])(=[O:16])=[O:17])([O-:18])(=[O:19])=[O:20].[nH+:21]1[cH:22][cH:23][cH:24][cH:25][cH:26]1.[nH+:27]1[cH:28][cH:29][cH:30][cH:31][cH:32]1>>[Br:1][c:2]1[cH:3][n:4]2[c:5]([s:6]1)[c:7]([CH:10]=[O:11])[n:8][cH:9]2

Participants

6

Reactant 5

HCID 6344DichloromethaneHCID 8857Ethyl AcetateHCID 24503Dichromate ionHCID 4989215Pyridinium2×HCID 591684062-Bromo-7-hydroxymethylimidazo[5,1-b]thiazole

Product 1

HCID 115287442-Bromoimidazo[5,1-b]thiazole-7-carbaldehyde

Sources & evidence

ORD record
ord-da40265bc58444ddb5056c9d46aa648f
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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