Sulfuric Acid → 3,4-Dimethoxy-5-nitrobenzhydrol

HRID 960796Notes

Reaction equation

HRID 960796 reaction equation
[CH3:8][O:9][c:10]1[cH:11][c:12]([CH:13]=[O:14])[cH:15][c:16]([N+:20](=[O:21])[O-:22])[c:17]1[O:18][CH3:19].[O:28]1[CH2:29][CH2:30][CH2:31][CH2:32]1.[S:23](=[O:24])(=[O:25])([OH:26])[OH:27].[c:1]1([Li:7])[cH:2][cH:3][cH:4][cH:5][cH:6]1>>[c:1]1([CH:13]([c:12]2[cH:11][c:10]([O:9][CH3:8])[c:17]([O:18][CH3:19])[c:16]([N+:20](=[O:21])[O-:22])[cH:15]2)[OH:14])[cH:2][cH:3][cH:4][cH:5][cH:6]1

Participants

5

Reactant 4

HCID 1118Sulfuric AcidHCID 8028TetrahydrofuranHCID 108675653,4-Dimethoxy-5-nitrobenzaldehydeHCID 178506676HCID 178506676, compound

Product 1

HCID 214589923,4-Dimethoxy-5-nitrobenzhydrol

Sources & evidence

ORD record
ord-869f7a8263ba419aa14b7d0963b78327
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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