Dichloromethane → 3-Triphenylmethyl-5-([4-[2-(4-methanesulfonyloxyphenyl)ethoxy]phenyl]methyl)oxazolidine-2,4-dione

HRID 960957Notes

Reaction equation

HRID 960957 reaction equation
[CH3:35][S:36](=[O:37])(=[O:38])[O:39][c:40]1[cH:41][cH:42][c:43]([CH2:46][CH2:47][OH:48])[cH:44][cH:45]1.[Cl:86][CH2:87][Cl:88].[N:49]([C:50]([N:51]1[CH2:52][CH2:53][CH2:54][CH2:55][CH2:56]1)=[O:57])=[N:58][C:59]([N:60]1[CH2:61][CH2:62][CH2:63][CH2:64][CH2:65]1)=[O:66].[c:1]1([C:7]([N:8]2[C:9](=[O:22])[O:10][CH:11]([CH2:14][c:15]3[cH:16][cH:17][c:18]([OH:21])[cH:19][cH:20]3)[C:12]2=[O:13])([c:23]2[cH:24][cH:25][cH:26][cH:27][cH:28]2)[c:29]2[cH:30][cH:31][cH:32][cH:33][cH:34]2)[cH:2][cH:3][cH:4][cH:5][cH:6]1.[c:67]1([P:68]([c:69]2[cH:70][cH:71][cH:72][cH:73][cH:74]2)[c:75]2[cH:76][cH:77][cH:78][cH:79][cH:80]2)[cH:81][cH:82][cH:83][cH:84][cH:85]1>>[c:1]1([C:7]([N:8]2[C:9](=[O:22])[O:10][CH:11]([CH2:14][c:15]3[cH:16][cH:17][c:18]([O:21][CH2:47][CH2:46][c:43]4[cH:42][cH:41][c:40]([O:39][S:36]([CH3:35])(=[O:37])=[O:38])[cH:45][cH:44]4)[cH:19][cH:20]3)[C:12]2=[O:13])([c:23]2[cH:24][cH:25][cH:26][cH:27][cH:28]2)[c:29]2[cH:30][cH:31][cH:32][cH:33][cH:34]2)[cH:2][cH:3][cH:4][cH:5][cH:6]1

Participants

6

Reactant 5

HCID 6344DichloromethaneHCID 11776TriphenylphosphineHCID 730421,1'-(Azodicarbonyl)dipiperidineHCID 149136625-(4-Hydroxybenzyl)-3-trityloxazolidine-2,4-dioneHCID 229887694-(2-Hydroxyethyl)phenyl methanesulfonate

Product 1

HCID 217049903-Triphenylmethyl-5-([4-[2-(4-methanesulfonyloxyphenyl)ethoxy]phenyl]methyl)oxazolidine-2,4-dione

Sources & evidence

ORD record
ord-7fd6435bda0d40f69daf1da3e2b81391
Source dataset
Validation data from https://doi.org/10.1039/C8SC04228D

Reaction notes

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