→ 283593-12-4

HRID 962322Notes

Reaction equation

HRID 962322 reaction equation
CC(=O)O.CCO.COC(=O)CC(C)=O.NC(N)=O.O.O=Cc1ccc(F)cc1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>COC(=O)C1=C(C)NC(=O)NC1c1ccc(F)cc1

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 3123384283593-12-4Yield 81%

Reagents, catalysts & solvents 6

HCID 176Acetic AcidOtherHCID 702EthanolOtherHCID 1176UreaOtherHCID 7757Methyl acetoacetateOtherHCID 680234-FluorobenzaldehydeOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. filtrationKeep solid
  3. washNo procedure recorded
  4. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-00a1b82def01418299554ed7d2bfc2c5
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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