→ HCID 10518006, compound

HRID 962339Notes

Reaction equation

HRID 962339 reaction equation
CC(=O)O.CCC(=O)CC(=O)OC.CCO.NC(N)=O.O.O=Cc1ccc(F)c(F)c1.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.O=S(=O)([O-])C(F)(F)F.[Yb+3]>>CCC1=C(C(=O)OC)C(c2ccc(F)c(F)c2)NC(=O)N1

Participants

7

Reactant 0

No Reactant data yet.

Product 1

HCID 10518006HCID 10518006, compoundYield 64%

Reagents, catalysts & solvents 6

HCID 176Acetic AcidOtherHCID 702EthanolOtherHCID 1176UreaOtherHCID 121699Methyl 3-oxovalerateOtherHCID 5880883,4-DifluorobenzaldehydeOtherHCID 45075687Ytterbium(3+) trifluoromethanesulfonate--water (1/3/1)Other

Conditions

Temperature
120 °C

Workup

  1. waitNo procedure recorded
  2. additionNo procedure recorded
  3. waitNo procedure recorded
  4. filtrationKeep solid
  5. washNo procedure recorded
  6. dry in vacuumNo procedure recorded

Sources & evidence

ORD record
ord-170115fea4834c9caeb6c43e61ea834e
Source dataset
Microwave-assisted Biginelli Condensation Dataset
Original link
View source

Reaction notes

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