HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19085499, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-(2-Bromoethoxy)-4-fluorobenzene | HCID 2064171 | — |
| Reactant | HCID 57180202 | HCID 57180202 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19085499 | HCID 19085499 | — |
Reaction Steps
In a similar manner to Example 3, a mixture of 4-(dimethylaminomethyliminomethyl)piperidine (6.42 g), 2-bromoethyl 4-fluorophenyl ether (8.3 g), triethylamine (5.3 ml) and toluene (20 ml) was heated on a steam bath for 16 hours to give 4-aminomethyl-1-[2-(4-fluorophenoxy)ethyl]piperidine as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05760035 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-86807b1052254b4099cce46545d4aecd |
| Source note | uspto-grants-1998_06 |