Hydrochloric Acid → HCID 86752685, compound

Participants

Reaction Steps

The product of step (c) above was dissolved in saturated methanolic hydrogen chloride, and allowed to stand at room temperature for 24 hours. The solvents were evaporated at reduced pressure then toluene was added to the residue and evaporated at reduced pressure to afford the title compound as a colourless foam. Analysis Calcd. for C23H23 F6NO3.HCl. 0.5(H2O): C, 53.03; H, 4.84; N, 2.69; Found: C, 52.78; H, 4.75; N, 2.75%. MS (Cl+) 476 (M+H)+.

Provenance & Evidence