Methylhydroquinone → HCID 19085794, compound

HRID 962637Notes

Reaction equation

HRID 962637 reaction equation
[CH3:1][C:2]1C=C(O)[CH:5]=[CH:6][C:7]=1[OH:8].[ClH:10].[CH2:11]([N:18]1[CH2:23][CH2:22][C:21](=O)[CH:20]([C:25]([O:27][CH2:28][CH3:29])=[O:26])[CH2:19]1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[ClH:10].[CH2:11]([N:18]1[CH2:23][CH2:22][C:21]2[C:1]3[CH:2]=[C:7]([OH:8])[C:6]([CH3:5])=[CH:29][C:28]=3[O:27][C:25](=[O:26])[C:20]=2[CH2:19]1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 7253MethylhydroquinoneHCID 102623Ethyl 1-benzyl-4-oxopiperidine-3-carboxylate hydrochloride

Product 1

HCID 19085794HCID 19085794, compoundYield 28%

Procedure

Prepared by the procedure of Example 1 from 3-methyl-4-hydroxyphenol and ethyl 1-benzyl-4-oxo-3-piperidinecarboxylate hydrochloride. The crude product was converted to the hydrochloride salt. Yield 28%; mp 283°-289° C.

Sources & evidence

ORD record
ord-c5a4d43ea5b94314b5a007a641759167
Source dataset
uspto-grants-1998_06
Patent number
US05760050

Reaction notes

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