4-Pyridinecarboxaldehyde → HCID 10567839, compound

HRID 962640Notes

Reaction equation

HRID 962640 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[C:16]3[CH2:15][CH2:14][NH:13][CH2:12][C:11]=3[C:10](=[O:17])[O:9][C:7]=2[CH:8]=1.[N:18]1[CH:23]=[CH:22][C:21]([CH:24]=O)=[CH:20][CH:19]=1>>[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]2[C:16]3[CH2:15][CH2:14][N:13]([CH2:24][C:21]4[CH:22]=[CH:23][N:18]=[CH:19][CH:20]=4)[CH2:12][C:11]=3[C:10](=[O:17])[O:9][C:7]=2[CH:8]=1

Participants

3

Reactant 2

HCID 133894-PyridinecarboxaldehydeHCID 131369188-Methoxy-1,2,3,4-tetrahydro-chromeno[3,4-c]pyridin-5-one

Product 1

HCID 10567839HCID 10567839, compoundYield 53%

Procedure

Prepared by the procedure of Example 3 from 8-methoxy-1,2,3,4-tetrahydro-chromeno[3,4-c]pyridin-5-one and 4-pyridinecarboxaldehyde. Yield 53%; mp 119°-122° C.

Sources & evidence

ORD record
ord-18183f06237743a1a98219d780cf71f5
Source dataset
uspto-grants-1998_06
Patent number
US05760050

Reaction notes

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