HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 131720700, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 131720702 | HCID 131720702 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 131720700 | HCID 131720700 | — |
Reaction Steps
Boc-Asp(OBzl)-Ser(Bzl)-OBzl (42.1 g) was dissolved in dioxane (100 ml), added with a solution of 4M-HCl/dioxane (150 ml) and stirred for 1 hour at room temperature. The reaction mixture was evaporated under reduced pressure and the residue was crystallized from ether to give Asp(OBzl)-Ser(Bzl)-OBzl hydrochloride (33.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763408 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-a2447e67b2394d2db3cdc78f94c12bcc |
| Source note | uspto-grants-1998_06 |