HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86752748, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 86752749 | HCID 86752749 | — |
| Product | HCID 86752748 | HCID 86752748 | 45.7% |
Reaction Steps
The title compound was prepared from cyclohexanecarboxylic acid (R)-[1-methyl-2-(4-thiophen-2-yl-3,6-dihydro-2H-pyrid-1-yl)-ethyl]-(pyrid-2-yl)-amide dihydrochloride (1.5 g, 3.6 mmol) and meta-chloroperbenzoic acid (0.632 g, 3.6 mmol) to yield 0.7 g of the title compound as the 1.8 hydrochloride, m.p. 109°-11° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763460 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-b8ff262fc8bd48c08bcd0d192b3c0ef1 |
| Source note | uspto-grants-1998_06 |