HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 23202566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Azepane | HCID 8119 | — |
| Reactant | 5-chloropentanal | HCID 643048 | — |
| Reactant | 1-[4-Acetylamino-5-chloro-2-(3,5-dimethoxybenzyloxy) phenyl)-5-chloropentan-1-one | HCID 19081830 | — |
| Product | HCID 23202566 | HCID 23202566 | — |
Reaction Steps
Proceeding as in Example 4, Step (c), but replacing 1-4-acetylamino-5-chloro-2-methoxyphenyl)-5-chloropentan-1-one with 1-[4-acetylamino-5-chloro-2-(3,5-dimethoxybenzyloxy) phenyl]-5-chloropentan-1-one and piperidine with azacycloheptane, gave 1-[4-amino-5-chloro-2-(3,5-dimethoxybenzyloxy) phenyl]-5-(azacyclohept-1-yl)pentan-1-one, m.p. 137°-139° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763458 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-9b393bdc072940b7893dc2b94ba0a0d6 |
| Source note | uspto-grants-1998_06 |