HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19081213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 19081266 | HCID 19081266 | — |
| Product | HCID 19081213 | HCID 19081213 | — |
Reaction Steps
A solution of l-acetoxymethyl-5,6,7,8-tetrahydro-isoquinoline (0.44 g) in 6N hydrochloric acid (10 ml) aqueous solution was heated for 4 hours at ca. 100° C. After cooling, the mixture was concentrated in vacuo to give 1-hydroxymethyl-5,6,7,8-tetrahydroisoquinoline hydrochloride (0.42 g) as a brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763437 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-a5346eff375f440cac1091cb328ff8b8 |
| Source note | uspto-grants-1998_06 |