Formic Acid → HCID 131720703, compound

Participants

Reaction Steps

The material from step b) (0.850 g) was dissolved in 80% formic acid (10 ml) and left to stand at room temperature for 22 hours. The mixture was partitioned between ether and water. The layers were separated and the aqueous layer extracted with ether. The ethereal extracts were combined, washed with brine, dried (MgSO4) and evaporated is under reduced pressure to yield the subtitled compound as an oil (0.70 g).

Provenance & Evidence