HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibromomethane → 4-Ethenylphenyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibromomethane | HCID 3024 | — |
| Reactant | Benzaldehyde, 4-(acetyloxy)- | HCID 70144 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-Ethenylphenyl acetate | HCID 75821 | — |
Reaction Steps
Then a mixture obtained by mixing 32.8 g of p-acetoxybenzaldehyde (PABA) (0.2 mol) and 52.15 g of dibromomethane (0.3 mol) in 85 g of anhydrous DMF was dropping for 1 hour keeping the internal temperature at 50° C. Then agitation was continued for 40 minutes under the same temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05763560 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-f5345871b7384f1f9277df1f844feb36 |
| Source note | uspto-grants-1998_06 |