HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 22117428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | 2-Isopropylphenol | HCID 6943 | — |
| Reactant | Hexane, 2,5-dichloro-2,5-dimethyl- | HCID 80360 | — |
| Product | HCID 22117428 | HCID 22117428 | — |
Reaction Steps
In a manner similar to Example 7(a) above, by the reaction of 30 g (0.22 mol) of 2-isopropylphenol with 40.3 g (0.22 mol) of 2,5-dichloro-2,5-dimethylhexane, 48.9 g (90%) of the expected phenol of melting point 79°-80° C. were obtained after chromatography on a silica column eluted with a mixture of dichloromethane and hexane (40/60).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05766610 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-017fc04e56f54368898e58b3c088e480 |
| Source note | uspto-grants-1998_06 |