Indole → HCID 67675945, compound
Reaction equation
[NH:1]1[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=[CH:2]1.[C:10]1([C:16]2([C:29]3[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=3)[O:20][C:19]3[CH:21]=[CH:22][C:23]([CH2:25][C:26](Cl)=[O:27])=[CH:24][C:18]=3[O:17]2)[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>>[C:29]1([C:16]2([C:10]3[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=3)[O:20][C:19]3[CH:21]=[CH:22][C:23]([CH2:25][C:26]([C:3]4[C:4]5[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=5)[NH:1][CH:2]=4)=[O:27])=[CH:24][C:18]=3[O:17]2)[CH:34]=[CH:33][CH:32]=[CH:31][CH:30]=1Participants
3
Procedure
The title compound was prepared by a similar method to that of Preparation 4 using indole and (2,2-diphenyl-1,3-benzodioxolan-5-yl)acetyl chloride (prepared from the corresponding carboxylic acid [see Preparation 7] by a similar method to that of Preparation 3) as the starting materials.
Workup
- customof Preparation 3) as the starting materials
Sources & evidence
- ORD record
- ord-f9f2f09dfe1a4ae2a323fb7984f0df2e
- Source dataset
- uspto-grants-1998_06
- Patent number
- US05767139
Reaction notes
Loading…