Hydrochloric Acid → HCID 19079193, compound

Participants

Reaction Steps

In 5 ml of methanol was dissolved 237 mg (0.792 mmol) of 2-amino-3-(2-(phthalimido)ethyl]pyridine. The solution was treated with 5 ml (10 mmol) of a 2N solution of hydrogen chloride in methanol. The solvent was distilled off to obtain the desired powder. The powder thus obtained was washed with ether to obtain 233 mg of the desired compound (yield: 79.0%, pale yellow powder).

Provenance & Evidence