2,8-Diacetylamino-1-tetralone → HCID 22449464, compound

Participants

Reaction Steps

The reaction was carried out in the same manner as in Example 1-(4), except that 250 mg of the compound prepared in (1) above was used instead of 2,8-diacetylamino-1-tetralone of Example 1-(4), and post-treated to produce 182 mg of the title compound. IRνmaxKBr cm-1 : 3428, 3336, 2216, 1652, 1614, 1542; NMR(CDCl3)δ: 1.6-2.0(1H, m), 2.09(3H, s), 2.56-3.39(3H, m), 4.51-4.71(1H, m), 6.59(1H, d, J=9.0 Hz), 7.40(1H, d, J=9.0 Hz); MASS m/z: 243(M+)

Provenance & Evidence