Hydrochloric Acid → HCID 357793, compound
Reaction equation
[CH3:1][O:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([OH:10])=[O:9].Cl.[CH3:12]O>>[CH3:1][O:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][C:8]([O:10][CH3:12])=[O:9]Participants
4
Procedure
6-Methoxy-caproic acid (6.17 g) was dissolved in dry methanol (90 ml) containing hydrogen chloride (catalytic amount) and held overnight at room temperature. The solvent was distilled off from the reaction solution under reduced pressure to give methyl 6-methoxy-caproate. Yield; 5.68 g
Workup
- distillationThe solvent was distilled off from the reaction solution under reduced pressure
Sources & evidence
- ORD record
- ord-948d68c20e84452abaebf341f1a3c3b2
- Source dataset
- uspto-grants-1998_06
- Patent number
- US05770759
Reaction notes
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