HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 21833062, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2-Acetyl-7-methoxy-4-benzofurancarboxylic acid | HCID 21833041 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21833062 | HCID 21833062 | — |
Reaction Steps
Intermediate 3 (0.12 g) was suspended in anhydrous dichloromethane (4 ml) at room temperature under nitrogen and oxalyl chloride (0.1 ml) added followed by 3 drops of N,N-dimethylformamide. Evaporation in vacuo after 2 hours afforded the title compound as a yellow solid (~0.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05773467 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-27c7595eebb04e1bb08e25e49e1c0f9d |
| Source note | uspto-grants-1998_06 |