反应详情

温度

70 °C

A mixture of nitrobenzophenone resin, 3-Scheme 6, (950 mg), NaSH (1.0 g) in THF (10 mL), MeOH (5 mL), water (5 mL) was heated in an oil bath at 70° C. for 16 h. The mixture was cooled, filtered and washed with methanol, water, methylene chloride and finally with methanol. Drying at 60° (in vacuo gave a slight yellow resin. Recovered (900 mg). IR 1640 (broad).

1. temperatureThe mixture was cooled
2. filtrationfiltered
3. washwashed with methanol, water, methylene chloride and finally with methanol
4. customDrying at 60° (in vacuo
5. customgave a slight yellow resin
6. customRecovered (900 mg)