HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → 1-Acetylindolin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Oxindole | HCID 321710 | — |
| Product | 1-Acetylindolin-2-one | HCID 323719 | — |
Reaction Steps
1,3-Dihydro-2H-indol-2-one (35.6 g, 0.268mol) suspended in acetic anhydride (30 ml) and mixture refluxed for 20 hours. Filtered and washed with diethyl ether (50 ml) dried in vacuo at 80° C. to give a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05773448 |
| Source dataset | uspto-grants-1998_06 |
| ORD ID | ord-17d447d27ed44c9cbb569ab43d61a717 |
| Source note | uspto-grants-1998_06 |