HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → 7,8-Dimethoxy-6-nitro-3-phenyl-chromen-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,4-Dimethoxy-2-hydroxy-5-nitrobenzaldehyde | HCID 22313432 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 7,8-Dimethoxy-6-nitro-3-phenyl-chromen-2-one | HCID 22313443 | — |
Reaction Steps
A mixture of 3,4-dimethoxy-2-hydroxy-5-nitrobenzaldehyde obtained from Preparation example (1a) (0.91 g), phenacetylchloride (1.1 ml) and potassium carbonate (2.0 g) was refluxed in dry acetone (40 ml) overnight. Acetone was evaporated, cold water added and filtered. Yield: 0.69 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951870B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-ac5eef07ca214db78624677c1de3aea9 |
| Source note | uspto-grants-2005_10 |