HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 69592045, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 69592076 | HCID 69592076 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 69592045 | HCID 69592045 | — |
Reaction Steps
Following the general method described in example 2b, 2-[2-(3,4-dichloro-phenyl)-vinyl]-pyridine 1-oxide was reacted first with dimethylsulfate and then with NaCN. After extraction and crystallization the title compound was obtained as a white crystalline material. Mp. 124-125° C. (hexane), MS: m/e=274 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951875B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-3b35021f2ac047e8abd9ccbc02e81132 |
| Source note | uspto-grants-2005_10 |