HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 69592051, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | HCID 69592043 | HCID 69592043 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 69592051 | HCID 69592051 | — |
Reaction Steps
Following the general method described in example 2b, 2-[2-(3-fluoro-phenyl)-vinyl]-pyridine 1-oxide was reacted first with dimethylsulfate and then with NaCN. After extraction and crystallization the title compound was obtained as a beige crystalline material. Mp. 111-112° C. (iPrOH), MS: m/e=224 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951875B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-23e897bac2584ebc94451d2e254bffbb |
| Source note | uspto-grants-2005_10 |