HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Mesityl-3-nitropyridine → 2-Mesityl-3-pyridinamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Mesityl-3-nitropyridine | HCID 22249491 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | 2-Mesityl-3-pyridinamine | HCID 16741426 | 106.5% |
Reaction Steps
Palladium-carbon (10%, 0.6 g) was added to a solution of 2-mesityl-3-nitropyridine (5.99 g, 23 mmol) in ethanol (120 mL), followed by stirring for one day in hydrogen atmospher. The mixture was filtered through Celite and evaporated, to give the title compound (5.2 g) as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06951865B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-c73ee1167547434ca4212285a5e42e77 |
| Source note | uspto-grants-2005_10 |