N-Methylallylamine → HCID 22314123, compound

HRID 966321Notes

Reaction equation

HRID 966321 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([Br:21])=[CH:17][CH:16]=3)=[C:13]([CH3:22])[S:12][C:11]=2[CH:23]=1.[CH2:24]([NH:27][CH3:28])[CH:25]=[CH2:26]>>[CH2:24]([N:27]([CH2:2][CH2:3][CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([Br:21])=[CH:17][CH:16]=3)=[C:13]([CH3:22])[S:12][C:11]=2[CH:23]=1)[CH3:28])[CH:25]=[CH2:26]

Participants

3

Reactant 2

HCID 69391N-MethylallylamineHCID 223139406-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-2-methyl-benzo[b]thiophene

Product 1

HCID 22314123HCID 22314123, compound

Procedure

According to the method in example 31, 6-(4-Bromo-butoxy)-3-(4-bromo-phenyl)-2-methyl-benzo[b]thiophene and Allyl-methyl-amine were converted to yield Allyl-{4-[3-(4-bromo-phenyl)-2-methyl-benzo[b]thiophen-6-yloxy]-butyl}-methyl-amine, MS: 444 (MH+, 1Br).

Sources & evidence

ORD record
ord-c5d544846b74443481e4eb0784a26a04
Source dataset
uspto-grants-2005_10
Patent number
US06951879B2

Reaction notes

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