HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 178483627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 178483624 | HCID 178483624 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178483627 | HCID 178483627 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-N-{2-[4-(3-chloro-(E)-propenyl)-cyclohexyl]-ethyl}-N-methyl-4-trifluoromethyl-benzenesulfonamide was reacted with piperidine in N,N-dimethylacetamide at room temperature to yield trans-N-methyl-N-{2-[4-(3-piperidin-1-yl-(E)-propenyl)-cyclohexyl]-ethyl}-4-trifluoromethyl-benzenesulfonamide as colorless viscous oil, MS: 473 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-ec0e64f4c0134dd6a57046432d689474 |
| Source note | uspto-grants-2005_10 |