HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylallylamine → HCID 178457228, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylallylamine | HCID 69391 | — |
| Reactant | HCID 178483623 | HCID 178483623 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178457228 | HCID 178457228 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-{2-[4-(3-chloro-(E)-propenyl)-cyclohexyl]-ethyl}-methyl-carbamic acid 4-chloro-phenyl ester was reacted with N-allyl-methyl-amine in N,N-dimethylacetamide at room temperature to yield trans-(2-{4-[3-(allyl-methyl-amino)-(E)-propenyl]-cyclohexyl}-ethyl)-methyl-carbamic acid 4-chloro-phenyl ester as light yellow viscous oil, MS: 405 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-41643eae08f64ccfab75a25c9dcc8e90 |
| Source note | uspto-grants-2005_10 |