HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyrrolidine → HCID 178483625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 178483623 | HCID 178483623 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 178483625 | HCID 178483625 | — |
Reaction Steps
In analogy to the method described in example 12.1, trans-{2-[4-(3-chloro-(E)-propenyl)-cyclohexyl]-ethyl}-methyl-carbamic acid 4-chloro-phenyl ester was reacted with pyrrolidine in N,N-dimethylacetamide at room temperature to yield trans-methyl-{2-[4-(3-pyrrolidin-1-yl-(E)-propenyl)-cyclohexyl]-ethyl}-carbamic acid 4-chloro-phenyl ester as yellow viscous oil, MS: 405 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06953806B2 |
| Source dataset | uspto-grants-2005_10 |
| ORD ID | ord-199d6644ae8448d1a278ebdc3fb9ef71 |
| Source note | uspto-grants-2005_10 |