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HRID967185

反应详情

EQUATION

反应方程式

HRID 967185 的结构方程式

REACTANTS

反应物

2
结构：C1CCNC1
HCID31268

Pyrrolidine

C4H9N

结构：CN(CC[C@H]1CC[C@H](/C=C/CCl)CC1)C(=O)Oc1ccc(Cl)cc1
HCID178483623

未命名化合物

PRODUCTS

生成物

1
结构：CN(CC[C@H]1CC[C@H](/C=C/CN2CCCC2)CC1)C(=O)Oc1ccc(Cl)cc1
HCID178483625

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)N(C)C
溶剂HCID31374

Dimethylacetamide

C4H9NO

PROCEDURE

实验过程

In analogy to the method described in example 12.1, trans-{2-[4-(3-chloro-(E)-propenyl)-cyclohexyl]-ethyl}-methyl-carbamic acid 4-chloro-phenyl ester was reacted with pyrrolidine in N,N-dimethylacetamide at room temperature to yield trans-methyl-{2-[4-(3-pyrrolidin-1-yl-(E)-propenyl)-cyclohexyl]-ethyl}-carbamic acid 4-chloro-phenyl ester as yellow viscous oil, MS: 405 (MH+, 1Cl).